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无水氯化锂

产品号 A10531 公司名称 Alfa Aesar
CAS号 7447-41-8 公司网站 http://www.alfa.com
分子式 ClLi 电 话
分子量 42.394 传 真
纯 度 98+% 电子邮件
保 存 Chembase数据库ID: 102979

产品价格信息

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产品别名

标题
Lithium chloride, anhydrous
IUPAC标准名
lithium(1+) ion chloride
IUPAC传统名
lithium(1+) ion chloride

产品登记号

EC号 231-212-3
CAS号 7447-41-8
MDL号 MFCD00011078
默克索引号 145528

产品性质

纯度 98+%
沸点 1325-1360°C
密度 2.068
熔点 605°C
GHS危险品标识 GHS06
GHS危险声明 H301-H315-H319-H335
欧盟危险性物质标志 X
GHS警示性声明 P261-P301+P310-P305+P351+P338-P302+P352-P405-P501A
危险公开号 22-36/37/38
RTECS编号 OJ5950000
安全公开号 26-36/37
保存注意事项 Hygroscopic
TSCA收录

产品详细信息

参考文献

  • In DMF, acts as a base in dehydrohalogenation reactions; see, for example: Org. Synth. Coll., 4, 162 (1963). See also lithium carbonate (preceding entry). A comparison has been made of its activity with or without microwave irradiation for promoting the Knoevenagel condensation in N-methylpyrrolidinone, e.g. of malononitrile: Chem. Commun., 773 (1998).
  • For use in the dealkylation of activated aralkyl ethers, see: Synthesis, 287 (1989).
  • In the Wadsworth-Emmons olefination reaction, Triethylamine, A12646, was effective as base in combination a number of metal salts of which Li halides gave the highest yields: J. Org. Chem., 50, 2624 (1985).
  • Additive in the Stille coupling reaction of alkyl and arylstannanes with aryl triflates, preventing decomposition of the palladium complex catalyst: J. Am. Chem. Soc., 106, 4630 (1984); 108, 3033 (1986); see also Tri-n-butyltin chloride, A10746.
  • The combination of LiCl and water in DMSO provides a mild and efficient method for deprotection of THP ethers: J. Org. Chem., 61, 6038 (1996), and ethylene acetals: Tetrahedron Lett., 38, 7271 (1997).