(3aS,7R,7aS)-7,7a-二氢-7-羟基-2,2-二甲基-1,3-苯并二氧戊环-4(3aH)-酮

• 产品号: 493880
• CAS号: 139013-57-3
• 分子式: C9H12O4
• 分子量: 184.18918
• 纯 度: 98%

产品别名

• 标题: (3aS,7R,7aS)-7,7a-Dihydro-7-hydroxy-2,2-dimethyl-1,3-benzodioxol-4(3aH)-one
• IUPAC标准名: (3aS,7R,7aS)-7-hydroxy-2,2-dimethyl-3a,4,7,7a-tetrahydro-2H-1,3-benzodioxol-4-one
• IUPAC传统名: (3aS,7R,7aS)-7-hydroxy-2,2-dimethyl-7,7a-dihydro-3aH-1,3-benzodioxol-4-one

产品登记号

• CAS号: 139013-57-3
• MDL号: MFCD01863551

产品性质

• 浓度: 0.2 g/mL in 0.1 M phosphate buffer
• Empirical Formula (Hill Notation): C9H12O4
• 纯度: 98%
• pH值: 8.5(adjusted to)
• 德国WGK号: 3

产品详细信息

详细说明 (English)

Reconstitution
To recover the pure product from the suspension:(1)Thaw the frozen suspension and filter the solid. (2) Rinse bottle with a few milliliters of base-washed (aqueous Na2CO3) ethyl acetate. (3) Use the rinsing to wash the solid. (4) Collect solid. (5) To further collect more product from the filtrate: extract filtratewith equal volumes of base-washed (aqueous Na2CO3) ethyl acetate (repeat three times). (6) Dry the ethyl acetate extract over MgSO4. (7) Evaporate the solvent - DO NOT HEAT! (8) Combine solids collected from the suspension and the filtrate. Pure crystals should be stored at -78° C. A suspension of the product in phosphate buffer is stable at 0° C.
Physical form
A suspension in phosphate buffer.

详细说明 (简体中文)

Reconstitution
要从悬浮液中回收纯产物：(1) 将冰冻悬浮液融化并过滤出固体。(2) 用几毫升碱性（含水 Na2CO3）乙酸乙酯洗液冲洗瓶子。(3) 用清水洗涤固体。(4) 收集固体。(5) 从滤出液中进一步收集更多产物：用等体积碱性（含水 Na2CO3）乙酸乙酯洗液抽提滤出液（重复三次）。(6) 将乙酸乙酯抽提物置于 MgSO4 上干燥。(7) 待溶剂蒸发-不要加热！(8) 合并从悬浮液和滤出液中收集的固体。纯晶体应保存于 -78°C。产物的磷酸盐缓冲液悬浮液在 0°C 时稳定。
Physical form
磷酸盐缓冲悬浮液。